Regulations last checked for updates: Jun 02, 2024

Title 40 - Protection of Environment last revised: May 30, 2024
§ 421.260 - Applicability: Description of the secondary precious metals subcategory.

The provisions of this subpart are applicable to discharges resulting from the production of precious metals at secondary precious metals facilities.

§ 421.261 - Specialized definitions.

For the purpose of this subpart:

(a) Except as provided below, the general definitions, abbreviations, and methods of analysis set forth in 40 CFR part 401 shall apply to this subpart.

(b) The term precious metals shall mean gold, platinum, palladium, rhodium, iridium, osmium, and ruthenium.

(c) The term Combined Metals, shall mean the total of gold, platinum and palladium.

[50 FR 38365, Sept. 20, 1985, as amended at 55 FR 31705, Aug. 3, 1990]
§ 421.262 - Effluent limitations guidelines representing the degree of effluent reduction attainable by the application of the best practicable control technology currently available.

Except as provided in 40 CFR 125.30 through 125.32, any existing point source subject to this subpart shall achieve the following effluent limitations representing the degree of effluent reduction attainable by the application of the best practicable technology currently available:

(a) Furnace wet air pollution control.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, incinerated or smelted
Copper136.40071.800
Cyanide (total)20.8208.616
Zinc104.80043.800
Ammonia (as N)9,571.0004,207.000
Combined metals21.54
Total suspended solids2,944.0001,400.000
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(b) Raw material granulation.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metal in the granulated raw material
Copper12.0506.340
Cyanide (total)1.8390.761
Zinc9.2563.867
Ammonia (as N)845.100371.500
Combined metals1.902
Total suspended solids259.900123.600
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(c) Spent plating solutions.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/liter of spent plating solution used as a raw material
Copper1.9001.000
Cyanide (total)0.2900.120
Zinc1.4600.610
Ammonia (as N)133.30058.600
Combined metals0.300
Total suspended solids41.00019.500
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(d) Spent cyanide stripping solutions.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by cyanide stripping
Copper7.0303.700
Cyanide (total)1.0730.444
Zinc5.4022.257
Ammonia (as N)493.200216.800
Combined metals1.110
Total suspended solids151.70072.150
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(e) Refinery wet air pollution control. 2

2 This allowance applies to either acid or alkaline wet air pollution control scrubbers. If both acid and alkaline wet air pollution control scrubbers are present in a particular facility the same allowance applies to each.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper39.90021.000
Cyanide (total)6.0902.520
Zinc30.66012.810
Ammonia (as N)2,799.0001,231.000
Combined metals6.300
Total suspended solids861.000409.500
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at alltimes.

(f) Gold solvent extraction raffinate and wash water.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by solvent extraction
Copper1.1970.630
Cyanide (total)0.1830.076
Zinc0.9200.384
Ammonia (as N)83.98036.920
Combined metals0.189
Total suspended solids25.83012.290
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(g) Gold spent electrolyte.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by electrolysis
Copper0.0170.009
Cyanide (total)0.0030.001
Zinc0.1030.005
Ammonia (as N)1.1600.510
Combined metals0.003
Total suspended solids0.3570.170
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(h) Gold precipitation and filtration.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold precipitated
Copper8.3604.400
Cyanide (total)1.2760.528
Zinc6.4242.684
Ammonia (as N)586.500257.800
Combined metals1.320
Total suspended solids180.40085.800
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(i) Platinum precipitation and filtration.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of platinum precipitated
Copper9.8805.200
Cyanide (total)1.5080.624
Zinc7.5923.172
Ammonia (as N)693.200304.700
Combined metals1.560
Total suspended solids213.200101.400
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(j) Palladium precipitation and filtration.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of palladium precipitated
Copper11.4006.000
Cyanide (total)1.7400.720
Zinc8.7603.660
Ammonia (as N)799.800351.600
Combined metals1.800
Total suspended solids246.000117.000
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(k) Other platinum group metals precipitation and filtration.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of other platinum group metals precipitated
Copper9.8805.200
Cyanide (total)1.5080.624
Zinc7.5923.172
Ammonia (as N)693.200304.700
Combined metals1.560
Total suspended solids213.200101.400
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(l) Spent solution from PGC salt production.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold contained in PGC product
Copper1.7100.900
Cyanide (total)0.2610.108
Zinc1.3140.549
Ammonia (as N)120.00052.740
Combined metals0.270
Total suspended solids36.90017.550
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(m) Equipment and floor wash.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper0.0000.000
Cyanide (total)0.0000.000
Zinc0.0000.000
Ammonia (as N)0.0000.000
Combined metals0.0000.000
Total suspended solids0.0000.000
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(n) Preliminary treatment.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of total precious metals produced through this operation
Copper95.00050.000
Cyanide (Total)14.5006.000
Zinc73.00030.500
Ammonia (as N)6665.0002930.000
Combined Metals15.000
Total Suspended Solids2050.000975.000
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

[50 FR 38365, Sept. 20, 1985, as amended at 55 FR 31705, 31706, Aug. 3, 1990]
§ 421.263 - Effluent limitations guidelines representing the degree of effluent reduction attainable by the application of the best available technology economically achievable.

Except as provided in 40 CFR 125.30 through 125.32, any existing point source subject to this subpart shall achieve the following effluent limitations representing the degree of effluent reduction attainable by the application of the best available technology economically achievable:

(a) Furnace wet air pollution control.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, incinerated or smelted
Copper5.7602.745
Cyanide (total)0.9000.360
Zinc4.5901.890
Combined metals1.350
Ammonia (as N)599.900263.700

(b) Raw material granulation.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals in the granulated raw material
Copper0.8190.390
Cyanide (total)0.1280.051
Zinc0.6530.269
Combined metals0.192
Palladium0.064
Platinum0.064
Ammonia (as N)85.31037.500

(c) Spent plating solutions.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/liter of spent plating solution used as a raw material
Copper1.2800.610
Cyanide (total)0.2000.080
Zinc1.0200.420
Gold
Combined metals0.300
Ammonia (as N)133.30058.600

(d) Spent cyanide stripping solutions.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by cyanide stripping
Copper4.7362.257
Cyanide (total)0.7400.296
Zinc3.7741.554
Combined metals1.110
Ammonia (as N)493.200216.800

(e) Refinery wet air pollution control 2.

2 This allowance applies to either acid or alkaline wet air pollution control scrubbers. If both acid and alkaline wet air pollution control scrubbers are present in a particular facility the same allowance applies to each.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper1.2800.610
Cyanide (total)0.2000.080
Zinc1.0200.420
Combined metals0.300
Ammonia (as N)133.30058.600

(f) Gold solvent extraction raffinate and wash water.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by solvent extraction
Copper0.8060.384
Cyanide (total)0.1260.050
Zinc0.6430.265
Combined metals0.189
Ammonia (as N)83.98036.920

(g) Gold spent electrolyte.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by electrolysis
Copper0.01110.0053
Cyanide (total)0.00170.0007
Zinc0.00890.0037
Combined metals0.0030
Ammonia (as N)1.16000.5100

(h) Gold precipitation and filtration.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold precipitated
Copper5.6322.684
Cyanide (total)0.8800.352
Zinc4.4881.848
Combined metals1.320
Ammonia (as N)586.500257.800

(i) Platinum precipitation and filtration.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of platinum precipitated
Copper6.6563.172
Cyanide (total)1.0400.416
Zinc5.3042.184
Combined metals0.560
Ammonia (as N)693.200304.700

(j) Palladium precipitation and filtration.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of palladium precipitated
Copper7.6803.660
Cyanide (total)1.200.480
Zinc6.1202.520
Combined metals1.800
Ammonia (as N)799.800351.600

(k) Other platinum group metals precipitation and filtration.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of other platinum group metals precipitated
Copper6.6563.172
Cyanide (total)1.0400.416
Zinc5.3042.184
Combined metals1.560
Ammonia (as N)693.200304.700

(l) Spent solutions from PGC salt production.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold contained in PGC product
Copper1.1520.549
Cyanide (total)0.1800.072
Zinc0.9180.378
Combined metals0.270
Ammonia (as N)120.00052.740

(m) Equipment and floor wash.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper0.0000.000
Cyanide (total)0.0000.000
Zinc0.0000.000
Combined metals0.000
Ammonia (as N)0.0000.000

(n) Preliminary treatment.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
Mg/troy ounce of total precious metals produced through this operation
Copper64.00030.500
Cyanide (Total)10.0004.000
Zinc51.00021.000
Combined metals15.000
Ammonia (as N)6665.0002930.000
[50 FR 38365, Sept. 20, 1985, as amended at 55 FR 31706, Aug. 3, 1990; 55 FR 36932, Sept. 7, 1990]
§ 421.264 - Standards of performance for new sources.

Any new source subject to this subpart shall achieve the following new source performance standards:

(a) Furnace wet air pollution control.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, incinerated or smelted
Copper5.7602.745
Cyanide (total)0.9000.360
Zinc4.5901.890
Combined metals1.350
Ammonia (as N)599.900263.700
Total suspended solids67.50054.000
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(b) Raw material granulation.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals in the granulated raw material
Copper0.8190.390
Cyanide (total)0.1280.051
Zinc0.6530.269
Combined metals0.192
Ammonia (as N)85.31037.500
Total suspended solids9.6007.680
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(c) Spent plating solutions.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/liter of spent plating solution used as a raw material
Copper1.2800.610
Cyanide (total)0.2000.080
Zinc1.0200.420
Combined metals0.300
Ammonia (as N)133.30058.600
Total suspended solids15.00012.000
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(d) Spent cyanide stripping solutions.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by cyanide stripping
Copper4.7362.257
Cyanide (total)0.7400.296
Zinc3.7741.554
Combined metals1.11
Ammonia (as N)493.200216.800
Total suspended solids55.50044.400
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(e) Refinery wet air pollution control 2.

2 This allowance applies to either acid or alkaline wet air pollution control scrubbers. If both acid and alkaline wet air pollution control scrubbers are present in a particular facility the same allowance applies to each.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper1.2800.610
Cyanide (total)0.2000.080
Zinc1.0200.420
Combined metals0.300
Ammonia (as N)133.30058.600
Total suspended solids15.00012.000
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(f) Gold solvent extraction raffinate and wash water.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by solvent extraction
Copper0.8060.384
Cyanide (total)0.1260.050
Zinc0.6430.265
Combined metals0.189
Ammonia (as N)83.98036.920
Total suspended solids9.4507.560
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(g) Gold spent electrolyte.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by electrolysis
Copper0.0110.005
Cyanide (total)0.0020.001
Combined metals0.003
Zinc0.0090.004
Ammonia (as N)1.1600.510
Total suspended solids0.1310.104
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(h) Gold precipitation and filtration.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold precipitated
Copper5.6322.684
Cyanide (total)0.8800.352
Zinc4.4881.848
Combined metals1.320
Ammonia (as N)586.500257.800
Total suspended solids66.0052.800
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(i) Platinum precipitation and filtration.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of platinum precipitated
Copper6.6563.172
Cyanide (total)1.0400.416
Zinc5.3042.184
Combined metals1.560
Ammonia (as N)693.200304.700
Total suspended solids78.00062.400
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(j) Palladium precipitation and filtration.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of palladium precipitated
Copper7.6803.660
Cyanide (total)1.2000.480
Zinc6.12002.520
Combined metals1.800
Ammonia (as N)799.800351.600
Total suspended solids90.00072.000
pH( 1)( 1)

1 Within the range of 7.5 to 10.00 at all times.

(k) Other platinum group metals precipitation and filtration.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of other platinum group metals precipitated
Copper6.6563.172
Cyanide (total)1.0400.416
Zinc5.3042.184
Combined metals1.560
Ammonia (as N)693.200304.700
Total suspended solids78.00062.400
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(l) Spent solution from PGC salt production.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold contained in PGC product
Copper1.1520.549
Cyanide (total)0.1800.072
Zinc0.9180.378
Combined metals0.270
Ammonia (as N)120.00052.740
Total suspended solids13.50010.800
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(m) Equipment and floor wash.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper0.0000.000
Cyanide (total)0.0000.000
Zinc0.0000.000
Combined metals0.000
Ammonia (as N)0.0000.000
Total suspended solids0.0000.000
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(n) Preliminary treatment.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of total precious metals produced through this operation
Copper64.00030.500
Cyanide (Total)10.0004.000
Zinc51.00021.000
Combined metals15.000
Ammonia (as N)6665.0002930.000
Total Suspended Solids750.000600.000
pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

[50 FR 38365, Sept. 20, 1985, as amended at 55 FR 31708, Aug. 3, 1990]
§ 421.265 - Pretreatment standards for existing sources.

Except as provided in 40 CFR 403.7 and 403.13, any existing source subject to this subpart which introduces pollutants into a publicly owned treatment works must comply with 40 CFR part 403 and achieve the following pretreatment standards for existing sources. The mass of wastewater pollutants in secondary precious metals process wastewater introduced into a POTW must not exceed the following values:

(a) Furnace wet air pollution control.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, incinerated or smelted
Copper5.7602.745
Cyanide (total)0.9000.360
Zinc4.5901.890
Combined metals1.350
Ammonia (as N)599.900263.700

(b) Raw material granulation.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals in the granulated raw material
Copper0.8190.390
Cyanide (total)0.1280.051
Zinc0.6530.269
Combined metals0.192
Ammonia (as N)85.31037.500

(c) Spent plating solutions.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/liter of spent plating solution used as a raw material
Copper1.2800.610
Cyanide (total)0.2000.080
Zinc1.0200.420
Combined metals0.300
Ammonia (as N)133.30058.600

(d) Spent Cyanide stripping solutions.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by cyanide stripping
Copper4.7362.257
Cyanide (total)0.7400.296
Zinc3.7741.554
Combined metals1.110
Ammonia (as N)493.200216.800

(e) Refinery wet air pollution control. 1

1 This allowance applies to either acid or alkaline wet air pollution control scrubbers. If both acid and alkaline wet air pollution control scrubbers are present in a particular facility the same allowance applies to each.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper1.2800.610
Cyanide (total)0.2000.080
Zinc1.0200.420
Combined metals0.300
Ammonia (as N)133.30058.600

(f) Gold solvent extraction raffinate and wash water.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by solvent extraction
Copper0.8060.384
Cyanide (total)0.1260.050
Zinc0.6430.265
Combined metals0.189
Ammonia (as N)83.98036.920

(g) Gold spent electrolyte.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by electrolysis
Copper0.0110.005
Cyanide (total)0.0020.001
Zinc0.0090.004
Combined metals0.003
Ammonia (as N)1.1600.510

(h) Gold precipitation and filtration.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold precipitated
Copper5.6322.684
Cyanide (total)0.8800.352
Zinc4.4881.848
Combined metals1.320
Ammonia (as N)586.500257.800

(i) Platinum precipitation and filtration.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of platinum precipitated
Copper6.6563.172
Cyanide (total)1.0400.416
Zinc5.3042.184
Combined metals1.560
Ammonia (as N)693.200304.700

(j) Palladium precipitation and filtration.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of palladium precipitated
Copper7.6803.660
Cyanide (total)1.2000.480
Zinc6.1202.520
Combined metals1.800
Ammonia (as N)799.800351.600

(k) Other platinum group metals precipitation and filtration.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of other platinum group metals precipitated
Copper6.6563.172
Cyanide (total)1.0400.416
Zinc5.3042.184
Combined metals1.560
Ammonia (as N)693.200304.700

(l) Spent solution from PGC salt production.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold contained in PGC product
Copper1.1520.549
Cyanide (total)0.1800.072
Zinc0.9180.378
Combined metals0.270
Ammonia (as N)120.00052.740

(m) Equipment and floor wash.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper0.0000.000
Cyanide (total)0.0000.000
Zinc0.0000.000
Combined metals0.000
Ammonia (as N)0.0000.000

(n) Preliminary Treatment.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
Mg/troy ounce of total precious metals produced through this operation
Copper64.00030.500
Cyanide (Total)10.0004.000
Zinc51.00021.000
Combined Metals15.000
Ammonia (as N)6665.0002930.000
[50 FR 38365, Sept. 20, 1985, as amended at 55 FR 31710, 31711, Aug. 3, 1990]
§ 421.266 - Pretreatment standards for new sources.

Except as provided in 40 CFR 403.7, any new source subject to this subpart which introduces pollutants into a publicly owned treatment works must comply with 40 CFR part 403 and achieve the following pretreatment standards for new sources. The mass of wastewater pollutants in secondary precious metals process wastewater introduced into a POTW shall not exceed the following values:

(a) Furnace wet air pollution control.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, incinerated or smelted
Copper5.7602.745
Cyanide (total)0.9000.360
Zinc4.5901.890
Combined metals1.350
Ammonia (as N)599.900263.700

(b) Raw material granulation.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, in the granulated raw material
Copper0.8190.390
Cyanide (total)0.1280.051
Zinc0.6530.269
Combined metals0.192
Ammonia85.31037.500

(c) Spent plating solutions.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/liter of spent plating solution used as a raw materail
Copper1.2800.610
Cyanide (total)0.2000.080
Zinc1.0200.420
Combined metals0.300
Ammonia (as N)133.30058.600

(d) Spent cyanide stripping solutions.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by cyanide stripping
Copper4.7362.257
Cyanide (total)0.7400.296
Zinc3.7741.554
Combined metals1.110
Ammonia (as N)493.200216.800

(e) Refinery Wet Air Pollution Control. 1

1 This allowance applies to either acid or alkaline wet air pollution control scrubbers. If both acid and alkaline wet air pollution control scrubbers are present in a particular facility the same allowance applies to each.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper1.2800.610
Cyanide (total)0.2000.080
Zinc1.0200.420
Combined metals0.300
Ammonia (as N)133.30058.600

(f) Gold solvent extraction raffinate and wash water.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by solvent extraction
Copper0.8060.384
Cyanide (total)0.1260.050
Zinc0.6430.265
Combined metals0.189
Ammonia (as N)83.98036.920

(g) Gold spent electrolyte.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by electrolysis
Copper0.0110.005
Cyanide (total)0.0020.001
Zinc0.0090.004
Combined metals0.300
Ammonia (as N)1.1600.510

(h) Gold precipitation and filtration.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold precipitated
Copper5.6322.684
Cyanide (total)0.8800.352
Zinc4.4881.848
Combined metals1.320
Ammonia (as N)586.500257.800

(i) Platinum precipitation and filtration.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of platinum precipitated
Copper6.6563.172
Cyanide (total)1.0400.416
Zinc5.3042.184
Combined metals1.560
Ammonia (as N)693.200304.700

(j) Palladium precipitation and filtration.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of platinum precipitated
Copper7.6803.660
Cyanide (Total)1.2000.480
Zinc6.1202.520
Combined Metals1.800
Ammonia (as N)799.800351.600

(k) Other platinum group metals precipitation and filtration.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of other platinum group metals precipitated
Copper6.6563.172
Cyanide (total)1.0400.416
Zinc5.3042.184
Combined metals1.560
Ammonia (as N)693.200304.700

(l) Spent solution from PGC salt production.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold contained in PGC product
Copper1.1520.549
Cyanide (total)0.1800.072
Zinc0.9180.378
Combined metals0.270
Ammonia (as N)120.00052.740

(m) Equipment and floor wash.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper0.0000.000
Cyanide (total)0.0000.000
Zinc0.0000.000
Combined metals0.000
Ammonia (as N)0.0000.000

(n) Preliminary treatment.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly averge
mg/troy ounce of total precious metals produced through this operation
Copper64.00030.500
Cyanide (Total)10.0004.000
Zinc51.00021.000
Combined Metals15.000
Ammonia (as N)6665.0002930.000
[50 FR 38365, Sept. 20, 1985, as amended at 55 FR 31711, Aug. 3, 1990]
§ 421.267 - [Reserved]
authority: Secs. 301, 304 (b), (c), (e), and (g), 306 (b) and (c), 307 (b) and (c), 308 and 501 of the Clean Water Act (the Federal Water Pollution Control Act Amendments of 1972, as amended by the Clean Water Act of 1977) and the Water Quality Act of 1987 (the “Act”); 33 U.S.C. 1311,1314,c,e,and, 1316 (b) andc, 1317 (b) andc,1318; 86 Stat. 816, Pub. L. 92-500; 91 Stat. 1567, Pub. L. 95-217; 101 Stat. 7, Pub. L. 100-4
source: 49 FR 8790, Mar. 8, 1984, unless otherwise noted.
cite as: 40 CFR 421.263